Hi all, here is the recipe for the alum...it was in an other forum I am in...
Re: REMOVING BROKEN TAP
« Reply #7 on 2/21/06 at 17:09 »
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Hello Folks,
to continue the saga of ''the broken Tap'', after the collective brain picking of this Forum and others, one in particular [the american horological society], the final result was to remove it with the use of ''ALUM'' i/e...aluminium potassium sulphate...this chemical is commonly used in the clock repair trade for removing rusted or broken screws from out of rare or antique clocks or watches when all else fails.
The process is slow but very sure as I have just proved.
During the tapping of a considerable number of 7ba threads, I managed to snap the Tap leaving approximately 3/8'' of broken tap in a blind hole.
The removal of the broken piece involved the use of a large sauce pan, a pyrex bowl, and 'ALUM', the pyrex bowl was filled with boiling water enough to cover the cylinder with broken tap by about 2'' of liquid, 'ALUM' powder was then poured into the bowl of boiling water until no more powder could be absorbed by the water, the bowl of liquid 'ALUM' was then put into the large saucepan which already had boiling water in it and left to simmer at just under boiling point for 15 hours over yesterday and today, that is what I mean by 'slow but sure', the gunmetal casting was not affected in any way and the remains of the broken tap had vanished.
It was amazing to watch the constant stream of tiny little bubbles erupting from hole where the broken bit of tap was being eaten away with the chemical.
For anyone who has never used this process before [like myself] I would heartily endorse it as an excellent ''MODEL ENGINEERS '' tool
and a little about ''ALUM''
''ALUM'' quite a few of us on occasion have had to use this substance, but how of its History...
1470: Alum (previously known in the Middle East) is discovered in Europe
for the first time, specifically Tuscany. It was first found between
1300 and 1310 in Rocca (Syria). The mineral Alum is
the double sulphate of aluminum and potassium, AlK(SO4)2 + 12 H2O,
is a common compound of Aluminum, which was not isolated until
1825 by Hans Christian Oersted (although anticipated and named in 1807
by Sir Humphrey Davy). Alum comes to be used for dyeing, leathermaking,
medicine, paper sizing, and fireproofing.
Europe's problem since Roman times had been a chronic imbalance of trade. Bullion drained out of northern Europe into Italy and thence through the Middle East to the Far East, to pay for imports of alum, grain, oil, and wine, and luxury goods like silk and pepper. In exceptional times and places this problem did not apply. For example, the fur and slave trade through Russia that was run by the Vikings and then by the Russians themselves resulted in a flow of silver north of the Black Sea into northern Europe. But this did not last for very long, and did not affect southern Europe very much. Venetian merchants were always reminding their agents in the east to use barter wherever they could, but they were usually required to pay in silver and gold; failing that, in copper, tin, or lead.
http://www.wovepaper.co.uk/alumessay1.html
Just a few snippets of its history, for those interested the web site gives an excellent review but a little long winded to down load...
All the best for now,
John.
« Last Edit: 3/27/08 at 9:44 by lancelot » Link